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Thermomechanical analyzer TMA 4000 SE
Thermomechanical analyzer TMA 4000 SE
Product details
The latest TMA 4000 SE thermal mechanical analyzer launched by Nike has excellent performance and high cost-effectiveness. Widely used for thermal expansion measurement in industries such as plastics, rubber, films, fibers, coatings, and composite materials.
TMA 4000 SE can be applied to:
Linear expansion and contraction, coefficient of thermal expansion (1/K)
• Volume expansion and contraction
Glass transition temperature (Tg)
• Softening temperature (Ts)
• Explosion temperature and explosion time
Expansion and contraction of powders and films
Thermal performance analysis of thermoplastic materials
Curing and Performance Analysis of Thermosetting Materials

Technical parameters of TMA 4000SE thermal mechanical analyzer:
• Temperature range:- 150 … 600°C
Heating rate: 0... 20 ° C/min
• Displacement range: ± 2500 μ m
• Displacement resolution: 2.5nm
• Stress range: 4.9N (0.98mN step size)
• Stress modes: compression/needle insertion, bending, tension
• Measurement atmosphere: oxidation, inertness, vacuum
• Refrigeration system: liquid nitrogen (optional)


TMA 4000 SE - Application Examples
Routine testing

Epoxy resin - expansion measurement
The sample undergoes a linear expansion process before approximately 60 ° C, with an expansion coefficient of 1.58 × 10-4 1/K. After 60 ° C, the sample undergoes glass transition and the coefficient of expansion changes.


Natural Spider Silk - Stretching Measurement
The spider silk sample measured in the picture has a diameter of only 1um.


Multilayer film samples - needle in measurement
In needle insertion mode, the two-layer film sample showed a two-stage needle insertion process. After penetrating one layer, the dL curve of the single-layer film sample has flattened.

Special testing

Resin curing test
The test is conducted in the form of oscillatory force. Compared to 25 ° C, 56 ° C has a lower initial viscosity and larger amplitude of the sample; But solidification occurs earlier, and as solidification occurs, the amplitude rapidly decreases.


Epoxy resin - fixed deformation testing
As the temperature increases, the natural expansion trend of the sample becomes larger, and the force required to maintain a fixed compression deformation also increases accordingly. It is not until the sample undergoes glass transition from 58 ° C that the modulus of the sample decreases and the required load force decreases accordingly.


Polyimide - Measurement of Expansion under Humidity Atmosphere
The blue TMA curve in the figure not only displays the corresponding thermal expansion of the sample as the constant temperature increases (from 20 ° C to 85 ° C), but also shows the corresponding hygroscopic expansion process as the ambient humidity increases (from 5% to 70%, 85% relative humidity).

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